In the sciences education, hands-on laboratory experiences are essential to the educational journey of students. These practical activities not only enrich the curriculum but also make learning more engaging and effective. By participating in laboratory experiments, students gain invaluable skills which can deepen their understanding of scientific concepts and enhance their overall science literacy.
In organic chemistry, handling common laboratory techniques is
crucial for successful experimentation. Skills such as reflux, simple
distillation, liquid-liquid extraction and recrystallization are fundamental to
the synthesis, isolation, purification and characterization of compounds.
However, many traditional organic chemistry experiments are often designed with
just one or two common techniques, which could hinder their comprehensive
understanding of basic laboratory techniques. This article introduces an
experiment designed to promote self-directed learning with pre-laboratory
preparation, allowing students to engage with a broader range of techniques in
organic synthesis.
Aims: To design an experiment focused on student self-directed
pre-laboratory preparation, utilizing a comprehensive approach that integrates
various laboratory techniques in organic reactions.
Study Design: A 2-hour
laboratory session was designed that systematically organizes several common
laboratory techniques, allowing students to practice these skills and perform
product identification analysis.
Place and Duration of Study: Department of Chemistry, Pui Ching
Middles School, between 2021 and 2022.
Methodology: 30 students work in groups of two. Benzophenone was
reduced by NaBH4. The reaction mixture was heated under reflux for
about five minutes. The product was then extracted by liquid-liquid extraction
and simple distillation. The crude product was purified by recrystallization
with hot hexane.
Results: The percentage yield of diphenylmethanol is about 68%.
Conclusion: The students experienced a series of laboratory skills
through the organic experiment. Through hands-on chemistry experiments,
students can investigate chemical properties and reactions by utilizing
laboratory apparatus and instruments.
Author
(s) Details
Tsz-Wing Wong
Pui Ching Middle School, Hong Kong, China.
Please see the book here:- https://doi.org/10.9734/bpi/rdcbr/v9/3166
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