Showing posts with label TEM. Show all posts
Showing posts with label TEM. Show all posts

Saturday, 10 May 2025

Novel PHEMA Nanoparticles for Controlled Drug Delivery: Synthesis, Characterization, and Potential Applications | Chapter 5 | Chemical and Materials Sciences: Research Findings Vol. 3

 

 

This chapter discusses the preparation and characterization of poly (2-hydroxyethyl methacrylate) (PHEMA) nanoparticles for potential use in controlled drug delivery. PHEMA nanoparticles were prepared using a modified suspension polymerization technique. This study describes the preparation, identification, and structural and morphological characterization of PHEMA nanoparticles. PHEMA nanoparticles have been characterized using Fourier Transform Infrared Spectroscopy (FTIR), scanning electron microscopy (SEM), and particle size analysis. FTIR is used to confirm the presence of specific functional groups within the PHEMA structure, while particle size distribution provides information about the dimensions and uniformity of the nanoparticles. It is found that the nanoparticles have having size of up to 100 nm and are almost identical in shape. The small size of nanoparticles makes them a suitable candidate for biomedical and pharmaceutical applications, especially in the controlled drug delivery field. PHEMA nanoparticles can encapsulate and release drugs, making them effective for targeted drug delivery, such as in cancer therapy. PHEMA nanoparticles are significant in biomedical applications due to their biocompatibility, tenable properties, and ability to serve as drug-delivery vehicles. Their high water content, low toxicity, and tissue compatibility make them suitable for a variety of medical devices and therapies, including soft contact lenses, drug delivery systems, and tissue regeneration scaffolds.

 

Author (s) Details

Huda Begam
Samrat Ashok Technological Institute, Vidisha (M.P), India.

 

A.K. Bajpa
Bose Memorial Research Laboratory, Department of Chemistry, Government Autonomous Science College, Jabalpur (MP)-482001, India.

 

Please see the book here:- https://doi.org/10.9734/bpi/cmsrf/v3/5316


Friday, 12 July 2024

Dielectric and Magnetic Properties of Nano-structure BaTiO3 Loaded with Sr: Co: Fe Ions; for Different Applications | Chapter 12 | Current Perspective to Physical Science Research Vol. 9

The current work inspiration is to progress the dielectric properties of perovskite nano-structure powder BaTiO3 designated as (BT*) triply-dope by 3 different transition elements (TE) such as; Sr, Fe and Co designated as (TDBTTE*). The following chemical compositions; Ba0.9Sr0.1TiO3, (Ba(1-x)SrxTiO3,) where (x=0.10) and (Ba 0.9Sr0.1 Ti(1-x-y)FexCoyO3), where (x=0.1,y=0) and (x=0 and y=0.10 ) and (x=0.5,y=0.5) designated as, (BST*) and (BST10FO*), (BST10CO*) and (BST5F5CO*), respectively were used in the samples preparation, then, heated at constant calcination temperature (CT*) 850oC. For dielectric measurement, the temperature range between 25˚C and 250˚C, respectively, and the dielectric range frequency between 42 Hz and 1 MHz was achieved. There is a sudden decrease in the (ε′) value for (BST*) and a rise in its value for (BST10CO*) and (BST5F5CO*), respectively. However, the addition of Fe3+ and Co2+ ions resulted in an increase in (ε′) of the (BST10FO*), (BST10CO*), and (BST5F5CO*) compared to the (BST*) host material at the same (CT*). These advancements in microstructure and firing density are thought to be connected to these modifications in dielectric characteristics. The (B10ST10C) exhibits the highest relative permittivity (ε') value.

The cited (TDBTTE*), which made by means of the (BT*) and (BST*) candidates as host materials for high-frequency ultrasonic and energy storage applications. A sudden decrease in the dielectric permittivity (DP*) by increasing the frequency range obtained for (TDBTTE*). The adapted sol-gel process (ASGP*) was employed in the sample’s preparation. The transmission electron microscope (TEM*) approves the prepared samples' nano-crystalline phase presence. Moreover, enrichment in the magnetization properties appeared by drawing the magnetic hysteresis loop. An increase in the saturation of the magnetization at room temperature was detected by reducing the crystallite sizes (CS*) of (TDBTTE*) which, we can consider promising candidates for energy storage, electrocaloric and spintronic applications.

Author(s) Details:

I.K. Battisha,
Solid State Physics Department, Physics Research Institute, National Research Centre (NRC), 33 El Behooth St., Dokki, Giza, Egypt and Electric and Dielectric Materials Measurement Unit, National Research Centre (NRC), 33 El Behooth St., Dokki, Giza, Egypt.

 


Please see the link here:
https://stm.bookpi.org/CPPSR-V9/article/view/14439

Saturday, 13 January 2024

Production of Ag and ZnO Nanoparticles Using Morinda citrifolia Extract and Comparison of Their Antibacterial Study of Nanoparticle-impregnated Jean Fabric | Chapter 8 | Advanced Concepts in Pharmaceutical Research Vol. 4

 Morinda citrifolia usually called as Noni belongs to Rubiaceae family was secondhand for synthesis of Ag and ZnO nanoparticles using green combination method. Morinda citrifolia (Noni) product juice is used as cure for several diseases in the way that arthritis, diabetics, high blood pressure, power aches and pains, menstrual problems, headaches, heart afflictions, AIDS, malignancy, gastric ulcers, sprains, mental despair, senility, poor digesting, atherosclerosis, blood vessel problems and drug hook. Noni has unique curative properties which help in normalization of unusually functioning cells by delivering the biography-chemical nutrients. Noni new fruits obtained from the forests present in the campus of GITAM, Visakhapatnam, India. Combined Ag and ZnO nanoparticles have been applied aware jean fabric by dip and cure method. Nanoparticles were from different methods in the way that UV- VISIBLE, FTIR, SEM, EDS, TEM and a comparative study of antimicrobial action were done. The happening of colour change in the nanoparticles was confirmed by UV – Spectroscopy. Identification of working groups in fruit which was being the reason for reduction of nanoparticles was observed by FTIR reasoning. The size and study of plants of the nanoparticles were observed by SEM and TEM. The presence of basic silver and zinc were rooted by EDS. The silver and zinc group of chemical elements nanoparticles synthesized using Noni product extract exhibited excellent inhibition against bacterial pathogens. Application of Ag and ZnO nanoparticles to jean material may reduce bacterial contaminations and blocks UV rays. Zone of hindrance of silver was almost akin to zinc group of chemical elements nanoparticles but comparative to silver, metallic mineral oxide was cost effective and less poisonous.

Author(s) Details:

Kantipriya Kondala,
Department of Biotechnology, College of Science, Dr. B R Ambedkar University, Etcherla, Srikakulam, Andhra Pradesh, India.

Sarvamangala Dhurjeti,
Department of Biotechnology, GIT, GITAM (Deemed to be University), India.

Sivakumar N.,
Department of Biochemistry, School of Life Science, University of Hyderabad, India.

Murthy U. S. N.,
Department of Ophthalmology, Gayatri Vidya Parishad Institute of Health Care and Medical Technology, Visakhapatnam, India.

Please see the link here: https://stm.bookpi.org/ACPR-V4/article/view/12929

Tuesday, 31 January 2023

Molecular Characterization and Epidemiology of Extended-spectrum-beta-lactamases in Clinical Isolates of Escherichia coli with Special Attention to CTX-M| Chapter 6 | Research Advances in Microbiology and Biotechnology Vol. 2

 This work shows that novel viruslike mesopore silicazinc group of chemical elements/Ag nanoparticles (SZnOAg) synthesized and professionally composed on NIR laser irradiation accompanying quercetin to improve the removal the mutated virus as a biomedical application. A singular type of silica nanoparticles with a selfinflating tubular surface has existed successfully combined using a novel singlemicelle epitaxial growth process. The characteristics of the nanoparticles can be brought into harmony with respect to their core width, tubular length, and external diameter. Due to their biomimetic presentation, they can rapidly transform living containers into virus-like pieces, this SZnOAg nanomaterial has specific elimination effect on bacteriophage and Covid-19. Using epitaxial development, we can construct bacterium-like structures that maybe used for biomedicine applications. These nanomaterials and NIR ray of light could prepare the way to a new range of antiviral materials, due to the lowefficiency basic uptake of current nanoparticles, their requests in the biomedical field are limited. Herein, it obviously shows that novel mesoporous silica nanoparticles can be easily shown superior cellular rude answer property.

Author(s) Details:

Nitika Anand,
Microbiology Department, I.T.S Dental College, Hospital and Research Centre, Greater Noida, India.

Please see the link here: https://stm.bookpi.org/RAMB-V2/article/view/9368

Tuesday, 21 June 2022

Investigation on Some Properties of Chemically Deposited Nanocrystalline CdZnS Compound- A Descriptive Study | Chapter 1 | New Trends in Physical Science Research Vol. 5

Chemical Method in Polyvinyl Alcohol (PVA) matrix solution at room temperature was used to develop nanocrystalline Cadmium Zinc sulphide (CdZnS) films onto cleaned glass substrates. The XRD method is employed to characterise the structure, and the investigation reveals the creation of nanoparticles that are smaller than CdS but larger than ZnS. The production of nanoparticles is also confirmed by transmission electron microscopy (TEM) images. The band gap energy of CdZnS is higher than that of CdS, according to an optical examination using a UV Spectrometer.


Author(s) Details:

P. K. Mochahari,
Department of Physics, Bodoland University, Kokrajhar, Assam, India.

Please see the link here: https://stm.bookpi.org/NTPSR-V5/article/view/7157

Wednesday, 16 March 2022

Experimental Investigation on the Characterization of HA/Alumina and HA/mgo Nanocomposites for Orthopedic Applications| Chapter 12 | Issues and Developments in Medicine and Medical Research Vol.11

 For the first time, HA/Alumina and HA/MgO nanocomposites were effectively produced at 250°C utilising the hydrothermal technique. In HA/Alumina and HA/MgO nanocomposites, the mechanisms of composite production, crystallite size, crystallinity, and shape were investigated. An intermolecular interaction between HA/Alumina and HA/MgO was discovered using XRD and FTIR techniques. The nature of the formation of HA/Alumina and HA/MgO nanocomposites is polycrystalline. The addition of magnesium to HAP promotes osteoblast growth. During the early phases of osteogenesis, magnesium functions like a growth factor, promoting bone production. TEM analysis confirmed it. HAP/Alumina was generated in a short nanorod shape, and HA/MgO nanocomposites have a nanocluster-like morphology, according to TEM images. The suitable vibrational spectra of HA/Alumina and HA/MgO nanocomposites can be seen using FTIR. The band–gap of HA/Alumina and HA/MgO nanocomposites is visible in UV–VIS experiments. This discovery lays the groundwork for future studies on HA/Alumina and HA/MgO nanocomposites for biomedical applications.

Author(s) Details:

V. Vijayalakshmi,
Erode Sengunthar Engineering College, Erode, India.


N. S. Mohan,
Erode Sengunthar Engineering College, Erode, India.

Please see the link here: https://stm.bookpi.org/IDMMR-V11/article/view/6084

Friday, 7 January 2022

Determination of Molecular Characterization of Extended Spectrum -Lactamase Genes in Clinical E. coli Isolates | Chapter 08 | New Visions in Science and Technology Vol. 11

 This study demonstrates that molecular characterisation and analytical approaches have a strong relationship. The genes that encode Extended Spectrum Beta-Lactamases (ESBLs) (TEM, SHV, and OXA) were amplified from multidrug-resistant E. coli. The plasmid encoded multidrug resistance E. coli isolates from various clinical sources were confirmed to be resistant to -lactam and cephalosporin. Seventy percent (70%) of the selected multi-drug resistant clinical isolates tested positive for ESBLs, with a 5 mm increase in zone diameter for either antibiotic relative to its zone when tested alone, according to conventional laboratory analysis. The antibiotic susceptibility test revealed that 100% of the isolates were resistant to amoxicillin-clavulanic acid, amoxicillin, cefuroxime, and ampicillin-sulbactam, while 90% were resistant to ceftazidine and tetracycline, 80% to ofloxacin, 70% to ceftriazon, nalidixic acid, cefalexin, 60% to ciprofloxacin, 50% to nitrofuranto The multiplex PCR with primers TEM (931bp), SHV (868), OXA-2 (478), aac(3)-IIa (900), and rmtA (634), which are genes responsible for extended spectrum -lactamase and aminoglycoside resistance in E. coli, shows that isolate W15 contains three (3) resistant genes, which correspond to TEM resolving as a 931 base pair, SHV 868 base pair, and a 4 Isolate B2 has a single resistant gene (478 base pair) that is interpreted as OXA-2, whereas isolates URO2, U64, and S45 have two resistance genes that resolve as 868 and 478 base pair, respectively, indicating SHV and OXA-2. Despite the varying degrees of antibiotic susceptibility profile test produced with traditional detection analysis, isolates S57, U58, and B7 revealed no gene amplification. Because these isolates are likely to contain other resistant genes that are also expressed at a molecular level, we assume that the primers utilised in this work do not code for their resistant genes.

 
Author(S) Details

James Chibueze Igwe
Department of Medical Biotechnology, National Biotechnology Development Agency, Abuja, Nigeria.

Josiah Ademola Onaolapo
Department of Pharmaceutics and Pharmaceutical Microbiology, Ahmadu Bello University, Zaria, Nigeria.

Mohammed Kachallah
Department of Pharmaceutics and Pharmaceutical Microbiology, University of Maiduguri, Maiduguri, Nigeria.

Amose Nworie
Department of Medical Laboratory Science, Ebonyi State University, Abakaliki, Nigeria.

Hannah Oluwakemi Oladipo
Department of Medical Biotechnology, National Biotechnology Development Agency, Abuja, Nigeria.

Beatrice Onyiye Ojiego
Department of Medical Biotechnology, National Biotechnology Development Agency, Abuja, Nigeria.

Obadiah Dauda Enose
Department of Medical Biotechnology, National Biotechnology Development Agency, Abuja, Nigeria.

Seyi Ebun Adeboye
Department of Medical Biotechnology, National Biotechnology Development Agency, Abuja, Nigeria.

Mojirayo Titilayo Durowaiye
Department of Pharmaceutical Microbiology, University of Ibadan, Ibadan, Nigeria.

Alex Uwadiegwu Akpa
Department of Medical Biotechnology, National Biotechnology Development Agency, Abuja, Nigeria.

Inimfon Akaninyene Ibanga
Department of Pharmaceutics and Pharmaceutical Microbiology, Ahmadu Bello University, Zaria, Nigeria.

View Book:- https://stm.bookpi.org/NVST-V11/article/view/5246

Thursday, 16 December 2021

Study on Synthesis, Characterization and Antituberculosis Activity of Biologically Nanostructured Zinc and Titanium Metal Compounds | Chapter 6 | New Innovations in Chemistry and Biochemistry Vol. 5

 Using an aqueous extract of horse gramme, green chemistry was employed to generate nano-range sized titanium and zinc compounds from their macro-sizes (Macrotyloma uniflorum). Through natural biological processes, green technology allows metal ions to be transformed into metal nanoparticles. The nanoparticles of biosynthesized metal nanoparticles were characterised using ultraviolet-visible (UV-vis) and Fourier-transform infrared (FTIR) spectrophotometers. The reduced nanoparticles of Ti and Zn metals were studied using transmission electron microscopy (TEM). In vitro features such as the effects of nano complex antimicrobials on Mycobacterium tuberculosis (MTB) H37RV strain were determined using micro dilution. Patients with multidrug-resistant tuberculosis (MDR-TB) had MTB strains that were resistant to first-line treatments. Antituberculosis activity was demonstrated in newly manufactured nano-complexes. In comparison to zinc nano complexes, titanium nano complexes had the highest minimum inhibitory concentration (MIC). In a cytotoxic research, both Ti and Zn nano complexes had an IC50 of 1000 g/mL, indicating that they were non-toxic when compared to isoniazid.


Author(S) Details

Savita Belwal
Department of Chemistry, Anurag Group of Institutions, Venkatapur, Ghatkesar, Hyderabad-500038, India.

Sujana Kariveda
Department of Chemistry, Anurag Group of Institutions, Venkatapur, Ghatkesar, Hyderabad-500038, India.

Saritha Ramagiri
Department of Chemistry, Anurag Group of Institutions, Venkatapur, Ghatkesar, Hyderabad-500038, India.

View Book:- https://stm.bookpi.org/NICB-V5/article/view/5147

Friday, 15 October 2021

Effect of Noble Metals (Ag, Au, Pt, Pd) loading over the Semiconducting p-NiO/ n-MoO3 Nanocomposite for Development of Green-House Gas Sensor | Chapter 6 | Recent Trends in Chemical and Material Sciences Vol. 3

 In light of the health risks linked with hazardous gases associated with industrial and car exhausts, global awareness of health and the environment is fast expanding. As a result, gas sensors are required to detect such dangerous chemicals, particularly greenhouse gases, in order to maintain the ecological balance. Semiconducting materials with nanostructured architecture have unique and appealing qualities such as high surface-to-volume ratio, high bandgap, small particle size, and so on, which are helpful for building sensitive and selective gas sensors. The design and production of a novel p-n type semiconducting MoO3: NiO nanocomposite functionalized by several noble metals (Ag, Au, Pt, and Pd) are described in this paper, with Pd integrated MoO3: NiO (MNPd) demonstrating superior efficiency compared to CO2 gas. The MoO3: NiO (MN) sensor had an outstanding sensitivity of S=80%, while the Pd-loaded MoO3: NiO (MNPd) sensor had an excellent sensitivity of S=96% and selectivity towards CO2 in comparison to other interfering gases. The findings clearly demonstrate the efficacy of the MNPd nanocomposite designed for a high-performance CO2 gas sensor.

Author (S) Details

G. Sarala Devi

Polymer and Functional Materials Division, CSIR-Indian Institute of Chemical Technology (CSIR-IICT), Habsiguda, Hyderabad – 500007, India. and 2Academy of Scientific and Innovative Research (AcSIR), Ghaziabad - 201002, India.

M. V. Manasa

Polymer and Functional Materials Division, CSIR-Indian Institute of Chemical Technology (CSIR-IICT), Habsiguda, Hyderabad – 500007, India. and 2Academy of Scientific and Innovative Research (AcSIR), Ghaziabad - 201002, India.



View Book :- https://stm.bookpi.org/RTCAMS-V3/article/view/4127

Friday, 6 August 2021

Determining the Template-Based Synthesis of Silica (SiO2-r) Rods and Its Corrosion Protection Performance | Chapter 5 | Newest Updates in Physical Science Research Vol. 10

 The cationic surfactant (cetyltrimethylammonium bromide) was utilised as a cationic surfactant, and ferric chloride (FeCl3) was used as an oxidant / structure-directing agent to make silica (SiO2-r) rods. To provide greater corrosion protection on mild steel, the SiO2-r rods were integrated into the acrylic-based matrix. To examine the surface morphology and composition, tests such as particle size, scanning electron microscopy, transmission electron microscopy, and Fourier-transform infrared spectroscopy were carried out. properties. Electrochemical impedance spectroscopy in a 3 percent NaCl solution was used to investigate corrosion prevention and coating durability. The addition of SiO2-r rods increased the acrylic coating matrix's corrosion resistance, according to the findings.


Author(s) Details

Dr. T. Siva
Laboratory for Advanced Research in Polymeric Materials, CIPET, Bhubaneswar - 751024, India.

P. Jayanthi

Research and Development Center, Bharathiar University, Coimbatore, 641046, India.

P. Thirumurugan
Research and Development Center, Bharathiar University, Coimbatore, 641046, India.

Dr. S. Sathiyanarayanan
CSIR-Central Electrochemical Research Institute, Karaikudi-630006, India.

A. Ayeshamariam
Department of Physics, KhadirMohideen College, Adirampattinam, 614701, India.

Professor M. Jayachandran
Department of Physics, Sethu Institute of Technology, Pulloor, Kariyapatti, 626115, Tamilnadu, India.

View Book :- https://stm.bookpi.org/NUPSR-V10/article/view/2378

Sunday, 1 August 2021

Cross-Sectional TEM Specimen Preparation for W/B4C Multilayer Sample Using FIB: A Recent Study | Chapter 7 | New Approaches in Engineering Research Vol. 8

 It is now possible to construct a cross-sectional transmission electron microscopy (TEM) specimen of a thin film multilayer sample using a cross-beam scanning electron microscopy (SEM)/focused-ion-beam (FIB) system, which was recently introduced.

A 300 layer pair thin-film multilayer sample of W/B4C was used to show the specimen lift-out approach, which took substantially less time than the traditional cross-sectional sample preparation technique. The FIB sample is followed by Ar+ ion polishing at 2 kV with grazing incidence to achieve a large area electron transparent sample. The prepared cross-sectional sample was examined using a transmission electron microscope.

Author (s) Details

Puspen Mondal
Raja Ramanna Centre for Advanced Technology, Indore, India.

View Book :- https://stm.bookpi.org/NAER-V8/article/view/2272

Saturday, 31 July 2021

Basics of Nanoscience, Nanomaterials and Nanotechnology | Book Publisher International

 The first chapter of this book begins with a definition of nano, nanoscale, and nanometer, as well as an introduction to the current period of Nanoscience, nanomaterials, and nanotechnology. The literature abstract is organised into parts and subsections and is provided as a sequential text. In summary, some examples have been used to demonstrate how bulk and nanomaterials differ based on the size of particles used as building blocks. The physical and chemical properties of the same substance in bulk and nanoform have been shown to fluctuate dramatically depending on particle size. There is also a distinction between nanoscience and nanotechnology. Nanomaterials are classified as 3D, 2D, 1D, and 0D materials due to the reduction in particle size (dimensions). It has been attempted to classify nanomaterials by accurately defining them with figures. The literature on what morphology is, how morphology helps to classify synthesised nanomaterials, and the usefulness of morphology for researchers and scientists to locate the right application field for synthesised nanomaterials can be found in the morphology section. In chapter 2, a brief introduction to electron microscopes, such as SEM and TEM, has been given to analyse the morphology of nanomaterials, and its detailed theory has been given. There are also some examples of nanomaterial morphology. Later in the manuscript, the merits and disadvantages of top-down and bottom-up methodologies for nanomaterial fabrication are discussed. The physical and chemical properties of nanomaterials have been briefly discussed as a function of particle size. The surface to volume ratio, quantum confinement, and reduced structural imperfection or flaws of nanomaterials are all stated. Then, a focus on particle size dependent physical properties of nanomaterials, such as structural, thermal, magnetic, optical, electronic, and electrical properties, as well as the causes for each property, was placed. By addressing specific numerical issues, distinctive properties of nanomaterials such as surface area to volume ratio and quantum confinement become prevalent when particle size decreases. After then, the nanocluster hypothesis was presented in full. The first chapter concluded with theory on 2D nanomaterials (Quantum wells), 1D nanomaterials (Quantum wires), and 0D nanomaterials (Nanoparticles - Nanoclusters, Quantum dots, and Buckyballs), as well as detailed theory on some special nanomaterials, such as fullerenes (0D nanomaterials), carbon nanotubes (1D nanomaterials), and graphene (2D nanomaterial). The second part of this book begins with an overview of nanotechnology, covering what it is, how it came to be, when the concept of nanotechnology became popular, its benefits, goals, and key elements. The gas (vapour) phase fabrication and liquid phase fabrication are highlighted as the two approaches that belong to the bottom-up approach after introducing two primary ways (top-down and bottom-up) for nanomaterial preparation. The theory of various methods for the synthesis of nanomaterials, such as chemical vapour deposition (CVD - Gas Phase Fabrication), Sol-gel method, and hydrolyzed colloid reaction (HCR) technique (wet chemical methods - Liquid Phase Fabrications), has been explained in detail under the heading of bottom-up approach. A thorough description of how to determine the particle size of nanomaterials using the BET theory and the Debye-Scherrer method for X-Ray diffraction patterns has been provided. Then, to examine the morphology and internal structure of nanomaterials, the s theory on electron microscopy, detail theory on scanning electron microscope (SEM), and transmission electron microscope (TEM) were introduced. The second chapter concluded with several applications of nanomaterials in various fields, nanotechnology issues, and numerical problems that were solved.


Author(s) Details

Upendra B. Mahatme
Department of Physics, K. Z. S. Science College, Bramnhi- Kalmeshwar, R.T.M. Nagpur University, India.

View Book:- https://stm.bookpi.org/BNNN/article/view/2483