Showing posts with label scanning electron microscopy. Show all posts
Showing posts with label scanning electron microscopy. Show all posts

Saturday, 14 March 2026

A Synthetic CAD-to-SEM Pipeline for Design-Based Semiconductor Defect Detection Using Structural Similarity Analysis | Chapter 3 | New Horizons of Science, Technology and Culture Vol. 9

 

The growing complexity of semiconductor manufacturing at advanced technology nodes has intensified the need for robust, automated defect inspection methods. Design-based inspection, which compares scanning electron microscope (SEM) images of fabricated wafers against their original computer-aided design (CAD) layouts, offers a powerful approach for detecting both systematic and random defects. However, the development and benchmarking of such inspection algorithms is severely constrained by the scarcity of labelled SEM defect datasets, which are expensive to produce and tightly guarded as proprietary by fabrication facilities. This chapter presents an end-to-end, open-source pipeline for generating synthetic paired CAD and SEM image datasets with controllable, ground-truth-labelled defects, and for performing automated defect detection through structural similarity (SSIM) analysis. The pipeline comprises five modular stages: (1) synthetic layout generation in industry-standard OASIS format, (2) paired CAD and SEM-like image rendering with physically motivated degradation models, (3) configurable synthetic defect injection, (4) phase-correlation-based image alignment followed by local SSIM computation and morphological post-processing for defect mask extraction, and (5) aggregate scoring and ranking of inspection sites by defect severity. The paired image rendering generates, for each inspection site, a clean binary CAD image and a SEM-like image with sequential physically motivated degradations simulating realistic electron microscopy effects. The defect injection module selectively modifies a configurable fraction of SEM images (default 10%) to introduce synthetic defects. The detection stage processes each matched pair of CAD and SEM images through four substeps: alignment, similarity mapping, thresholding, and morphological cleanup. Experimental results on a generated dataset of 200 image pairs demonstrate that the pipeline achieves a detection F1-score of 0.93 under moderate noise conditions and degrades gracefully as imaging noise increases. The fully reproducible, configurable nature of this toolkit makes it suitable for algorithm benchmarking, machine learning model pre-training, threshold optimisation studies, and educational demonstrations of semiconductor inspection concepts.

 

 

Author(s) Details

Balachandar Jeganathan
ASML, San Jose, CA, USA.

 

Please see the book here :- https://doi.org/10.9734/bpi/nhstc/v9/7212

Monday, 26 May 2025

Investigation of Nonlinear Absorption Coefficient of rGO-Incorporated ZnO: Al Composite Thin Film by Z-Scan Technique | Chapter 12 | Current Research Progress in Physical Science Vol. 9

Graphene, a single-layer, two-dimensional nanomaterial, has gained significant attention in various scientific and technological fields due to its remarkable properties. Its exceptional optical, mechanical, thermal, and electronic characteristics make it highly suitable for applications in optoelectronics and photonics. The fabrication of a reduced graphene oxide (rGO)-integrated aluminum-doped zinc oxide (ZnO: Al) composite thin film on a glass substrate using the spin coating technique has been presented. In this study, rGO/ZnO: Al thin films were fabricated on thoroughly cleaned glass substrates using the spin coating technique. Reduced graphene oxide (rGO) was synthesized using a modified Hummer’s method. The influence of rGO on the structural and linear optical characteristics of the rGO/ZnO: Al composite film was examined through X-ray powder diffraction (XRD), Scanning Electron Microscopy (SEM) and UV-Vis absorption spectroscopy. Structural analysis confirmed the presence of a hexagonal wurtzite structure, with strong interfacial bonding between rGO and ZnO: Al. The incorporation of rGO led to a redshift in the band gap energy of ZnO: Al. The nonlinear absorption behavior of the composite thin film was investigated using the open-aperture Z-scan technique with a Q-switched Nd: YAG laser at 532 nm. The Z-scan results revealed that the composite film exhibits reverse saturable absorption, with a nonlinear absorption coefficient (β) of 5.93 × 10-5 cm/W. The incorporation of rGO leads to a decrease in the ZnO: Al diffraction peak intensity, which can be linked to the reduction of ZnO content in the composite. These findings highlight the potential of rGO/ZnO: Al thin films for applications in absorbing-type optical devices, including optical limiters, optical switches, and optical sensor protection in the field of nonlinear optics. In conclusion, the incorporation of rGO enhances exciton formation in ZnO: Al, leading to improved linear absorption and band gap modulation. Open-aperture Z-scan measurements reveal the presence of reverse saturable absorption (RSA), primarily driven by two-photon absorption (TPA) and free carrier absorption (FCA).

 

Author (s) Details

V.G Sreeja
Department of Physics and Centre for Research, St. Teresa’s College (Autonomous), Ernakulam, Kerala – 682011, India.

 

S. Rekha
Department of Physics, Maharajas College, Ernakulam, Kerala – 682011, India.

 

E.I Anila
Christ, (Deemed to be University) Bangalore -560029, India.

 

Please see the book here:- https://doi.org/10.9734/bpi/crpps/v9/5141

Saturday, 3 May 2025

Investigation of Nonlinear Absorption Coefficient of rGO-Incorporated ZnO: Al Composite Thin Film by Z-Scan Technique | Chapter 10 | Current Research Progress in Physical Science Vol. 9

Graphene, a single-layer, two-dimensional nanomaterial, has gained significant attention in various scientific and technological fields due to its remarkable properties. Its exceptional optical, mechanical, thermal, and electronic characteristics make it highly suitable for applications in optoelectronics and photonics. The fabrication of a reduced graphene oxide (rGO)-integrated aluminum-doped zinc oxide (ZnO: Al) composite thin film on a glass substrate using the spin coating technique has been presented. In this study, rGO/ZnO: Al thin films were fabricated on thoroughly cleaned glass substrates using the spin coating technique. Reduced graphene oxide (rGO) was synthesized using a modified Hummer’s method. The influence of rGO on the structural and linear optical characteristics of the rGO/ZnO: Al composite film was examined through X-ray powder diffraction (XRD), Scanning Electron Microscopy (SEM) and UV-Vis absorption spectroscopy. Structural analysis confirmed the presence of a hexagonal wurtzite structure, with strong interfacial bonding between rGO and ZnO: Al. The incorporation of rGO led to a redshift in the band gap energy of ZnO: Al. The nonlinear absorption behavior of the composite thin film was investigated using the open-aperture Z-scan technique with a Q-switched Nd: YAG laser at 532 nm. The Z-scan results revealed that the composite film exhibits reverse saturable absorption, with a nonlinear absorption coefficient (β) of 5.93 × 10-5 cm/W. The incorporation of rGO leads to a decrease in the ZnO: Al diffraction peak intensity, which can be linked to the reduction of ZnO content in the composite. These findings highlight the potential of rGO/ZnO: Al thin films for applications in absorbing-type optical devices, including optical limiters, optical switches, and optical sensor protection in the field of nonlinear optics. In conclusion, the incorporation of rGO enhances exciton formation in ZnO: Al, leading to improved linear absorption and band gap modulation. Open-aperture Z-scan measurements reveal the presence of reverse saturable absorption (RSA), primarily driven by two-photon absorption (TPA) and free carrier absorption (FCA).

 

Author (s) Details

V.G Sreeja
Department of Physics and Centre for Research, St. Teresa’s College (Autonomous), Ernakulam, Kerala – 682011, India.

 

S. Rekha
Department of Physics, Maharajas College, Ernakulam, Kerala – 682011, India.

 

E.I Anila
Christ, (Deemed to be University) Bangalore -560029, India.

 

 Please see the book here:- https://doi.org/10.9734/bpi/crpps/v9/5141

Thursday, 24 April 2025

Effectiveness of Household Water Filtration Systems in Eliminating Plastic Particles: A Case Study from Mosul City, Iraq | Chapter 2 | Geography, Earth Science and Environment: Research Highlights Vol. 10

On a global scale, plastic particles are a concern. The presence of microplastics (MPs) in tap water is becoming a global issue because of the risks associated with human consumption and health impacts on humans. Providing clean, safe drinking water may be challenging when MPs are present in drinking water, considered emerging pollutants. This study aimed to assess the presence and characteristics of MPs and to evaluate the removal efficiency (RE%) of household water filter systems (HWFS). The research was carried out in 12 sites in Mosul City. The identification of microplastics, as well as the morphological characterization (color, shape, and size) and analysis of polymer types, was performed by stereomicroscope, scanning electron microscopy (SEM) and Fourier transform spectroscopy (FTIR) techniques. The study revealed that the effectiveness of HWFS was between 93% and 30%, depending on several variables such as the age of the filter and the number of its stages. Fibers and fragments were the dominant morphotypes, comprising about 94% of all analyzed MPs. The transparent color accounting for about 52 % of the overall. Roughly 35% of MPs sizes were smaller than 10 µm. Around 58% of all considered polymer types corresponded to polyvinyl chloride (PVC), which was the highest percentage.  In addition, PVC had the highest risk index compared to the other polymer types.

 

Author (s) Details

 

Raghad N. Altaee
Department of Environmental Technologies, College of Environmental Sciences, University of Mosul, Mosul, 41002, Iraq.

 

Kossay K. Al-Ahmady
Ministry of Higher Education and Scientific Research, Baghdad, 10011, Iraq.

 

Rasha Khalid Sabri Mhemid
Department of Environmental Technologies, College of Environmental Sciences, University of Mosul, Mosul, 41002, Iraq.

 

 

Please see the book here:- https://doi.org/10.9734/bpi/geserh/v10/5015

 

Wednesday, 19 February 2025

Synthesis, Characterization and Potential Applications of Exfoliated Graphite/ABS Composites | Chapter 4 | Engineering Research: Perspectives on Recent Advances Vol. 3

Exfoliated graphite has received attention as a filler in composites in recent times due to the prominent properties it imparts to the host polymeric matrices. In this study, exfoliated graphite was created using a chemical method, followed by thermal oxidation and sonication to reduce its size and increase the spacing between its layers. To explore its potential applications, composites of exfoliated graphite and acrylonitrile butadiene styrene (ABS) were prepared with different filler concentrations using a simple solution casting technique. Synthesis of exfoliated graphite involves chemical treatment of thermal exfoliation for the formulation and reduction of graphite oxide. Various analytical tools, including scanning electron microscopy (SEM), energy dispersive X-ray analysis (EDAX), Fourier transform infrared (FTIR) spectroscopy, and X-ray diffractometry (XRD), were used to characterize the materials. The results showed that thermal exfoliation was successful, as indicated by the disappearance of the main graphite peak at 2θ = 26.4°. SEM images confirmed the uniform distribution of exfoliated graphite within the ABS matrix, while EDAX results demonstrated that the graphite oxide had been effectively reduced. Exfoliated graphite was successfully obtained through thermal exfoliation reduction reaction which was confirmed by SEM and EDAX analysis. Treatment of the natural flake graphite resulted in size reduction and an increase in interlayer spacing of exfoliated graphite as confirmed by XRD.

 

Author (s) Details

Bhardwaj Neha
Central Institute of Plastics Engineering and Technology, Ahmedabad, India.

 

K. S. Manjula
Central Institute of Plastics Engineering and Technology, Ahmedabad, India.

 

B. Srinivasulu
Central Institute of Plastics Engineering and Technology, Ahmedabad, India.

 

Shit C. Subhas
Central Institute of Plastics Engineering and Technology, Ahmedabad, India.

 

Please see the book here:- https://doi.org/10.9734/bpi/erpra/v3/4013

Saturday, 13 January 2024

Synthesis of Uniform and Strongly Adherent Poly (Aniline-co-o-toluidine) Copolymer Coatings on Copper | Chapter 3 | Current Innovations in Chemical and Materials Sciences Vol. 4

 The uniform and powerfully adherent poly(aniline-co-o-toluidine) (PAOT) copolymer coatings were synthesized on law enforcement officer (Cu) by the electrochemical copolymerization of aniline accompanying o-toluidine. Also the individual polymer i.e. polyaniline (PANI) and polytoluidine (Cauldron) coatings were synthesized on Cu under cyclic voltammetric environments. Aqueous oxalate answers were used as the supporting electrolytes for the combining of PAOT, PANI and POT coatings on Cu. The happening coatings were characterized by different spectroscopic methods, cyclic voltammetry, ultraviolet–visible absorption spectroscopy, Fourier translate infrared spectroscopy (FTIR), basic magnetic resonance spectroscopy (NMR), and flipping through electron microscopy. The comparative study of description results was carried out of PAOT5, Container and PANI coatings.The Fourier Transform Infra Coral (FTIR) spectroscopy and Nuclear Magnetic Reverberation (NMR) spectroscopy studies reveal that the copolymerization of aniline and o-toluidine takes establish Cu substrates from an aqueous oxalate solutions and happening in PAOT copolymer, there are more o-toluidine wholes than aniline units.

Author(s) Details:

Pritee Raotole,
MGSM’s Arts, Science and Commerce College, Chopda, Dist-Jalgaon 425107, Maharashtra, India.

S. R. Patil,
MGSM’s Arts, Science and Commerce College, Chopda, Dist-Jalgaon 425107, Maharashtra, India.

Please see the link here: https://stm.bookpi.org/CICMS-V4/article/view/12932

Saturday, 3 June 2023

Physicomechanical and Morphological Structure Analysis on the Oil-heat Treated 10 Years Tectona grandis | Chapter 12 | Research Highlights in Science and Technology Vol. 3

 This paper checked properties that focussed on the microphotographs form, physical properties, and machinelike characterization of the heat-medicated 10-year-traditional cultivated Tectona grandis forest. The harvested wood was commit the heat treatment process at 160°C, 200°C, and 240°C for two hours in an electrically stimulate oil heat-situation machine. The heat-acted and the control untreated samples were subsequently unprotected in the two (2) age grave-yard tests ground. Selected teak forest was taken out after sustaining a certain ending of testing. Moreover, the material properties, to a degree the moisture content, maximum density, fundamental density, and volumetric decrease were determined. The machinelike properties were evaluated using static turning and compression tests concentrating on the modulus of elasticity (MOE) and modulus of rupture (MOR). The physicomechanical test was completed activity according to the ASTM standard.  The study revealed that the lubricate heat-treatment process changed the cell form of the teak wood, specifically at those exposed to elevated hotnesses. Changes were observed in the fibre and parenchyma containers of the wood, and the heat situation process generally improved the characteristics of the wood, specifically in the physical characteristics. The Scanning Electron Microscope (SEM) was used to study changes in the wood's plants and microstructures especially on treated, not cooked, and ground test samples. The study results showed that the lubricate heat-treatment process revised the durability of teak forest against wood-decaying fungi. Nonetheless, extreme heat situation temperatures changed the teak wood's containers’ structure, leading to discounted strength in the container walls but at an satisfactory level.

Author(s) Details:

Mohamad Saiful Sulaiman,
Centre of Excellence in Wood Engineered Products, University of Technology Sarawak (UTS), Sibu 96000, Sarawak, Malaysia and University of Technology Sarawak (UTS), Sibu 96000, Sarawak, Malaysia.

Razak Wahab,
Centre of Excellence in Wood Engineered Products, University of Technology Sarawak (UTS), Sibu 96000, Sarawak, Malaysia and University of Technology Sarawak (UTS), Sibu 96000, Sarawak, Malaysia.

Sofiyah Mohd Razali,
Centre of Excellence in Wood Engineered Products, University of Technology Sarawak (UTS), Sibu 96000, Sarawak, Malaysia.

Hashim W. Samsi,
Forest Research Institute Malaysia (FRIM), Malaysia.

Ros Syazmini Mohd Ghani,
Centre of Excellence in Wood Engineered Products, University of Technology Sarawak (UTS), Sibu 96000, Sarawak, Malaysia and University of Technology Sarawak (UTS), Sibu 96000, Sarawak, Malaysia.

Taharah Edin,
Centre of Excellence in Wood Engineered Products, University of Technology Sarawak (UTS), Sibu 96000, Sarawak, Malaysia and University of Technology Sarawak (UTS), Sibu 96000, Sarawak, Malaysia.

Nasihah Mokhtar,
Centre of Excellence in Wood Engineered Products, University of Technology Sarawak (UTS), Sibu 96000, Sarawak, Malaysia and University of Technology Sarawak (UTS), Sibu 96000, Sarawak, Malaysia.

Please see the link here: https://stm.bookpi.org/RHST-V3/article/view/10763

Wednesday, 1 March 2023

Determining the Effect of Zno Nano Particles against Escherichia coli Strains | Chapter 5 | Current Overview on Pharmaceutical Science Vol. 7

 An attempt was made to study antibacterial activity of ZnO nanoparticles on Gram-negative bacteria, E. coli. By using scanning electron microscopy (SEM), X-ray diffraction (XRD), and ultraviolet (UV) analysis, zinc oxide nanoparticles were characterised. Different zinc oxide nanoparticle concentrations were used in the antimicrobial study, which was carried out using well diffusion assays and growth rate studies. Effect of nano particles on bacterial growth was determined by comparing growth curves of the ZnO treated and untreated bacterial cultures.

The results showed zinc oxide nanoparticles to be an effective bactericide. Scanning electron microscopy was used to study the bactericidal action of these nano scale materials. The zinc oxide nanoparticles were discovered to have accumulated in the bacterial membrane while the treated E. coli cells displayed damages by the formation of "pits" in the bacterial cell wall. Such a membrane's morphology causes a marked increase in permeability, which kills the cell. DNA changes were detected using atomic force microscopy on bacterial DNA that had been exposed to nanoparticles. The presented strategy opens up wide applications in various fields like optical switches, shutters, waveguides, and optical filters and in biomedical applications. The adopted synthetic procedure is amenable to fine tune the properties of the particles produced by choosing the suitable constituents at molecular level.

Author(s) Details:

Anju Thangam,
Department of Biotechnology, SRM University, Kattankulathur, Kancheepuram-603 203, Tamil Nadu, India.

. Pritam,
Department of Biotechnology, SRM University, Kattankulathur, Kancheepuram-603 203, Tamil Nadu, India.

Sakthi Ramlakshmi,
Department of Biotechnology, SRM University, Kattankulathur, Kancheepuram-603 203, Tamil Nadu, India.

Please see the link here: https://stm.bookpi.org/COPS-V7/article/view/9696



Wednesday, 4 May 2022

Microstructure Properties of Decay in Chemically Treated Tropical Bamboo (Gigantochloa scortechinii) via Electron Microscopy| Chapter 4 | Research Developments in Science and Technology Vol. 3

This chapter focused on the anatomical characteristics and microstructures of Gigantochloa scortechinii, a three-year-old tropical bamboo species. The bamboo culms were chosen at random and felled from forest bamboo stands controlled by the Forest Research Institute Malaysia (FRIM), with the age of each culm appropriately marked. The bamboo culms were chopped at a height of around 30 cm above the ground. At DBH, all culms had diameters ranging from 10 to 12 cm. Before being transferred to the workshop and subsequent laboratories, the cut surface was painted with an end-coating paint. The efficiency of the selected chemicals and their application procedures in treating the bamboo culms was investigated using electron microscopy with high magnification. At the level of tissue cells, the scanning electron microscope was employed extensively, whereas the transmission electron microscope was used at the level of cell walls. The study focused on tissue such as vascular bundles, fibres, parenchyma, and regions in the middle lamella situated at the internodes and nodes of chemically treated bamboo culms at the bottom, middle, and top of the bamboo culms at the middle cross sections. The untreated bamboo culms were used as a comparison. While the properties of bamboo culms remained stable as they grew higher, their morphological elements and microstructure changed, according to the research. The discrepancies between SEM and TEM micrographs were also examined by the researchers.


Author(s) Details:

Razak Wahab,
Centre of Excellence in Wood Engineered Products (CeWEP), 96000 Sibu, Sarawak, Malaysia and  University of Technology Sarawak (UTS), 96000 Sibu, Sarawak, Malaysia.

Mohamad Saiful Sulaiman,
Centre of Excellence in Wood Engineered Products (CeWEP), 96000 Sibu, Sarawak, Malaysia and  University of Technology Sarawak (UTS), 96000 Sibu, Sarawak, Malaysia.

Sofiyah Mohd Razali,
Centre of Excellence in Wood Engineered Products (CeWEP), 96000 Sibu, Sarawak, Malaysia.

Nasihah Mokhtar,
Centre of Excellence in Wood Engineered Products (CeWEP), 96000 Sibu, Sarawak, Malaysia and  University of Technology Sarawak (UTS), 96000 Sibu, Sarawak, Malaysia.

Taharah Edin,
Centre of Excellence in Wood Engineered Products (CeWEP), 96000 Sibu, Sarawak, Malaysia and  University of Technology Sarawak (UTS), 96000 Sibu, Sarawak, Malaysia.

Ros Syazmini Mohd Ghani,
Centre of Excellence in Wood Engineered Products (CeWEP), 96000 Sibu, Sarawak, Malaysia and University of Tasmania, Launceston, TAS 7250, Australia.

Please see the link here: https://stm.bookpi.org/RDST-V3/article/view/6629

Monday, 9 August 2021

Description of an Anatomical Structure and Changes of Microstructure through the Grave Yard Test on Treated and Untreated Three-Year-Old Gigantochloa scortechinii via Electron Microscopy | Chapter 8 | Current Approaches in Science and Technology Research Vol. 11

 The microstructures of a variety of tropical bamboo species were studied. Three-year-old Gigantochloa scortechinii were harvested and separated into various places and postures. Through the vacuum pressure, sap displacement, and soaking technique, bamboo samples were treated with copper-chrome-arsenic (CCA), ammonia-copper-quaternary (ACQ), and a borax-boric-acid (BBA). Electron Microscopy (EM), particularly Scanning Electron Microscope (SEM) and Transmission Electron Microscope (TEM), is then used to examine the samples' microstructure. For SEM and TEM, the coating process and spurr resin techniques were used. The changes in vascular bundles, fibres, and parenchyma cells at the internodes and nodes, as well as the exterior, middle, and inner sections of natural and preservative-treated bamboos, were studied. The properties of the bamboo species were found to be comparable, while the anatomical aspects and microstructure were found to be distinct. This research also uses SEM and TEM micrographs to show the impacts of treated and untreated samples in a ground contact test.


Author (S) Details

Mohamad Saiful Sulaiman
University College of Technology Sarawak (UCTS), 96000 Sibu, Sarawak, Malaysia and Centre of Excellence in Wood Engineered Products, UCTS, 96000 Sibu, Sarawak, Malaysia.

Razak Wahab
University College of Technology Sarawak (UCTS), 96000 Sibu, Sarawak, Malaysia and Centre of Excellence in Wood Engineered Products, UCTS, 96000 Sibu, Sarawak, Malaysia.

Mohammad Haziq Razak
Universiti Sains Malaysia (USM), Penang, Malaysia.

Nasihah Mokhtar
University College of Technology Sarawak (UCTS), 96000 Sibu, Sarawak, Malaysia and Centre of Excellence in Wood Engineered Products, UCTS, 96000 Sibu, Sarawak, Malaysia.

Taharah Edin
University College of Technology Sarawak (UCTS), 96000 Sibu, Sarawak, Malaysia and Centre of Excellence in Wood Engineered Products, UCTS, 96000 Sibu, Sarawak, Malaysia.

Ros Syazmini Mohd Ghani
University College of Technology Sarawak (UCTS), 96000 Sibu, Sarawak, Malaysia and University of Tasmania, Australia.

View Book :- https://stm.bookpi.org/CASTR-V11/article/view/2457